Name is 2,3-Dihydro-1,4-benzodioxine-6-carboxylic acid, as a common heterocyclic compound, it belongs to benzodioxans compound, and cas is 4442-54-0, its synthesis route is as follows.,4442-54-0
The 2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylic acid (9.0 g, 50 mmol) was dissolved in anhydrous ethanol (50 mL) containing concentrated H2SO4 (5 mL), which were refluxed overnight. The solvent was evaporated until no longer liquid outflow. Water (20 mL) was added, extracting by adding respectively 40, 30 and 20 mL ethyl acetate. The organic phases were sequentially washed with saturated NaHCO3, brine, and dried over MgSO4. The solvent was removed under reduced pressure to yield compound 2.
With the complex challenges of chemical substances, we look forward to future research findings about 2,3-Dihydro-1,4-benzodioxine-6-carboxylic acid
Reference£º
Article; Yan, Ru; Zhang, Zhi-Ming; Fang, Xian-Ying; Hu, Yang; Zhu, Hai-Liang; Bioorganic and Medicinal Chemistry; vol. 20; 4; (2012); p. 1373 – 1379;,
Benzodioxan
1,4-Benzodioxane | C8H8O2 – PubChem